3-(2-吡啶基)-1,2,4-三唑衍生物的合成  

Synthesis of 3-(pyridin-2-yl)-1,2,4-triazole derivatives

作　　者：张俊珺[1,2] 张春华[1] 阳年发[2] 何华平[2] 李碧辉[2] 

机构地区：[1]衡阳师范学院化学与材料科学系,湖南衡阳421008 [2]湘潭大学环境友好化学与应用省部共建教育部重点实验室,湖南湘潭411105

出　　处：《化学研究与应用》2010年第6期749-753,共5页Chemical Research and Application

基　　金：湖南省教育厅重点项目(07A013)资助;湖南省重点建设学科项目资助;湖南省教育厅-有机功能材料重点实验室项目资助;衡阳师院博士启动基金项目资助

摘　　要：3-(pyridin-2-yl)-1,2,4-triazole was synthesized through two steps from the raw material 2-cyanopridine,and a series of derivatives(3a～3d)which were reported in this paper were synthesized by the reaction of 3-(pyridin-2-yl)-1,2,4-triazole with(o-,m-,p-)2-chloro-methyl pyridine.Their structures were characterized by elementary analyses,IR,1H NMR and 13C NMR.3-（pyridin-2-yl）-1,2,4-triazole was synthesized through two steps from the raw material 2-cyanopridine,and a series of derivatives（3a～3d）which were reported in this paper were synthesized by the reaction of 3-（pyridin-2-yl）-1,2,4-triazole with（o-,m-,p-）2-chloro-methyl pyridine.Their structures were characterized by elementary analyses,IR,1H NMR and 13C NMR.

关 键 词：2-氰基吡啶 氯甲基吡啶 3-(2-吡啶基)-1 2 4-三唑 合成 

分 类 号：O626.26[理学—有机化学]