美研醇的合成研究  

Synthesis of Majantol

作　　者：阮礼波 刘烽[2] 欧文华[2] 毛海舫[2] 潘仙华[2] 

机构地区：[1]上海香料研究所,上海200234 [2]上海应用技术学院香料香精技术与工程学院,上海200235

出　　处：《上海应用技术学院学报（自然科学版）》2010年第1期64-67,共4页Journal of Shanghai Institute of Technology: Natural Science

摘　　要：美研醇具有清新、柔软、强烈的百合花香,是配制透发型铃兰香精的关键原料,目前对此化合物的合成报道较少。以间二甲苯作为起始原料,经过溴代、烷基化、还原等反应得到了美研醇,总收率达55.7%。对合成的产物结构,利用1H NMR、IR和GC-MS等手段进行表征。Majantol has a powerful floral,fresh and green flowery perfume and lily of the valley note.Few papers were published on the synthesis of majantol.In this paper majantol was synthesized from m-xylene,via bromination,alkylation and reduction in a total yield of 55.7%.And the products were determined by 1H NMR,IR and GC-MS.

关 键 词：美研醇 铃兰香气 合成 

分 类 号：TQ655[化学工程—精细化工]