2,3-二氰基丙酸乙酯的气相色谱分析  

Determination of Ethyl 2,3-dicyanopropionate by GC

作　　者：杨漫波 游霞[1] 王海容[1] 

机构地区：[1]四川省天然气化工研究院,成都610212

出　　处：《四川化工》2010年第3期40-42,共3页Sichuan Chemical Industry

摘　　要：建立了气相色谱法测定2,3-二氰基丙酸乙酯含量的分析方法。选用邻苯二甲酸二甲酯为内标物,以内标标准曲线法作为定量方法进行分析测定,方法的线性相关系数r为0.9992,方法精密度为0.34%,加标回收率为98.13%-101.65%。该方法的灵敏度高、操作简单、定量准确、重现性好,可用于生产中2,3-二氰基丙酸乙酯产品的检测。The analysis method of the ethyl 2,3-dicyanopropionate was established with the gas chromatography（GC） in this paper.Dimethyl（o-） phthalate was selected as internal standard substance,and the quantitative method was internal standard curve method,the correlation coefficient r was 0.9992,the accuracy of the method as RSD was 0.34%,and the average recovery was 98.13%～101.65%.This method is found to be sensitive,simple,accurate and reproducible,and it can be used for the determination of 2,3-dicyanopropionate in production.

关 键 词：2 3-二氰基丙酸乙酯 气相色谱 内标标准曲线法 

分 类 号：TQ225.241[化学工程—有机化工]