扩散条件下抽拉速率对Fe-4.2Ni合金定向凝固组织演化的影响  

EFFECTS OF PULLING RATE ON MICROSTRUCTURE EVOLUTION OF DIRECTIONALLY SOLIDIFIED Fe-4.2Ni ALLOY IN DIFFUSION REGIME

作　　者：冯周荣[1] 沈军[1] 王伟[1] 闵志先[1] 傅恒志[1] 

机构地区：[1]西北工业大学凝固技术国家重点实验室,西安710072

出　　处：《金属学报》2010年第3期311-317,共7页Acta Metallurgica Sinica

基　　金：国家自然科学基金项目50774061;凝固技术国家重点实验室自主研究课题项目28-TP-2009资助~~

摘　　要：在内径为1 mm的细管中进行了Fe-4.2Ni亚包晶合金扩散条件下的定向凝固实验.在15μm/s抽拉速率下得到了树状组织、共生组织以及δ/γ两相分离生长的凝固组织,组织演化规律为:δ单相→δ/γ两相树状组织→γ+两相共生组织→δ/γ两相分离并列生长组织;抽拉速率为35μm/s时,获得了以γ岛状为主的凝固组织,组织演化规律为:δ单相→δ/γ两相树状组织→γ-岛状组织+共生组织→δ+γ-岛状组织.实验发现,提高抽拉速率使凝固初始阶段的两相生长竞争加剧,并导致凝固过程中的相选择和全程组织演化规律发生改变.Phase selection and microstructure evolution play important roles on processing and property control of the materials with peritectic reactions.Many interesting microstructures,such as peritectic coupled growth（PCG）,discrete banding,island banding（IB） and oscillatory tree-like structure were observed in directionally solidified peritectic alloys.In recent years,a number of theoretical models have been developed for the phase selection.For example,it was believed that peritectic coupled growth is initiated by island banding and is similar to eutectic coupled growth, discrete banding is shaped by nucleation and lateral spreading of one phase onto the other phase,and island banding is formed when the nucleation rate of one phase on the other phase growth interface is higher than a critical value,and etc..But these models were developed under the assumption that the growth of the phases are controlled by diffusion only,whereas the actual experimental studies were mainly carried out in bulk metallic samples with the presence of convection.Although it has been believed that the convection effects on microstructure evolution are very important and could not be neglected,studies were seldom carried out in diffusive regime.In this paper, directional solidification of Fe-4.2Ni hypo-peritectic alloy in diffusive regime was carried out in a Bridgman furnace by placing the samples in 1 mm inner diameter thin tubes.The experimental results show that various microstructures and phase selections are obtained in the directionally solidified thin samples at the pulling rates of 15 and 35μm/s.Tree-like structure,peritectic coupled growth and the steadily solidified structure of two phases separated growth are formed at the pulling rate of 15μm/s,and the microstructures evolution is：single phaseδ→tree-like structure→γand PCG→separately growingδ/γ.At the pulling rate of 35μm/s,the main microstructure isγ-IB,and the microstructures evolution is：δ→tree-like structure→γ-IB in the center and PCG at the edg

关 键 词：FE-NI合金 扩散 定向凝固 组织演化 

分 类 号：TG113.12[金属学及工艺—物理冶金]