(E+Z)-2-[2-(4-N′-甲基-N′-甲烷磺酰基苯)-1-(4-氟苯)二苯甲酮基]-N-芳基-联氨羰草酰胺衍生物的合成  

Synthesis of (E+Z)-2-[2-(4-N′-methyl -N′- methanesulfonyl phenyl)-1-(4- fluorophenyl)Benzophenone]-N- aryl- hydrazine Carbonyl Oxamide Derivatives

作　　者：刘永榜[1] 孔小林[2] 彭伟立[2] 沈德隆[1] 邢家华[2] 陈杰[2] 夏旭建[2] 

机构地区：[1]浙江工业大学农药研究所,杭州310014 [2]浙江省化工研究院有限公司,浙江杭州310023

出　　处：《浙江化工》2010年第7期1-3,共3页Zhejiang Chemical Industry

摘　　要：为了寻求新的含缩氨基脲先导化合物,以对硝基苯甲酰氯,氟代苯,甲烷磺酰氯,水合肼、苯基异氰酸酯等为原料合成得到一类新的(E+Z)-2-[2-(4-N′-甲基-N′-甲烷磺酰基苯)-1-(4-氟苯)二苯甲酮基]-N-芳基-联氨羰草酰胺衍生物。对所得化合物结构均经1HNMR和MS表征。In order to find new semicarbazone lead compounds, （E ＋Z）-2-[2-（4-N＇-methyl -N＇- methanesulfonyl phenyl）-1-（4- fluorophenyl）Benzophenone]-N- aryl- hydrazine carbonyl oxamide derivatives were synthesized by 4-nitrobenzoyl chloride, fluorobenzene, methanesulfuryl chloride,hydrazine hydrate, phenylisoeyanates,etc. The structures of the products were characterized by ^1H NMR and MS.

关 键 词：二苯甲酮腙 缩氨基脲 合成 杀虫剂 

分 类 号：TQ453.2[化学工程—农药化工]