联立方程组新解法测定复方益康宁二组分含量  被引量:3

New Solution Pertinent to Simultaneous Equations for Determination of Procaine Hydrochloride and VB_6 in Compound “Yikangning”Tablets

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作  者:叶青[1] 黄河舟[1] 骆望美[1] 

机构地区:[1]海军医学高等专科学校药物分析教研室,南京210099

出  处:《海军医高专学报》1999年第2期73-75,共3页

摘  要:目的:测定复方益康宁中的盐酸普普卡因和维生素B6二组分含量。方法:采用光度分析中的联立方程组新解法测定盐酸普鲁卡因和维生素B6二组分含量。结果:在选定的实验条件下盐酸普鲁卡因和维生素B6的线性范围分别是0.000-0.147mmol/L和0.000-0.175mmol/L。该两组分的回收率分别为100.5%和99.8%,CV不大于1.9%(n=10)。结论:本方法用吸收比代替吸收系数,不但操作简便而且准确度高。Objective:To detendne the amounls of procaine HCl and vitamin B6 in compound 'Yikangning' tablets. Methods: A new solution to simultaneous equations (Vierordt's method) in spec- trophotometry was used to determine the contents of procaine HCl and vitamin B, in the compound tablets. Results: Under the selected experimental condition, the calibration concentration of procaine HCl and vi- tandn B, was within the linear range of 0 .000- 0.147 mmol/L and 0 .000- 0.175 mmol/L, respective- ly. The rates of recovery were 100 .5% for procaine HCl and 99. 8 % for vitawhn B, with CV not more than 1 .9 % (n =10). Conclusion: The new method is used for replacing the absorPtion coefficients with the absorPtion ratios, and it is not only simple but also accurate.

关 键 词:Vierordt法 盐酸普鲁卡因 维生素B6 复方益康宁 

分 类 号:R927.2[医药卫生—药学]

 

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