4-(2-(4-(苄氧基)苯氧基)乙氧基)-1,2,3-丁三醇结构的核磁共振鉴定  

Identification of 4-(2-(4-(Benzyloxy)Phenoxy)Ethoxy) Butane-1,2,3-Triol by Nuclear Magnetic Resonance

作　　者：杨扬[1] 孙小强[1] 尹芳华[1] 席海涛[1] 于树林[1] 

机构地区：[1]常州大学江苏省精细化工重点实验室,江苏常州213164

出　　处：《常州大学学报（自然科学版）》2010年第2期1-4,共4页Journal of Changzhou University：Natural Science Edition

基　　金：国家自然科学基金项目资助(20872051)

摘　　要：采用一维的氢谱、碳谱、无畸变极化转移增强谱和二维氢-氢、碳-氢、空间相关核磁共振技术,对4-(2-(4-(苄氧基)苯氧基)乙氧基)-1,2,3-丁三醇的结构进行了表征,确定了4-(2-(4-(苄氧基)苯氧基)乙氧基)-1,2,3-丁三醇1H、13C NMR谱峰的归属。The chemical structure of 4-（2-（4-（benzyloxy）phenoxy）ethoxy）butane-1,2,3-triol was identified by means of nuclear magnetic resonance spectral analysis.With the aid of one dimensional（including 1H,13C-NMR and distortionless enhancement by polarization transfer） and two dimensional NMR techniques（including 1H-1H correlation spectroscopy,1H-13C correlation spectroscopy and nuclear Overhauser effect spectroscopy）,the full assignment of 1H and 13C NMR spectral data were presented.

关 键 词：4-(2-(4-(苄氧基)苯氧基)乙氧基)-1 2 3-丁三醇 核磁共振 结构鉴定 

分 类 号：O657.2[理学—分析化学]