草豆蔻中元素测定及索氏法提取的挥发油化学成分分析  

Studies on elements and determination of chemical component of volatile oil extracting by Soxhelt methods in alpinia katsumadai hayata

作　　者：陈少东[1] 陈福北[1] 卢平[1] 陈剑平 刘红星[3] 聂坤梅[1] 

机构地区：[1]广西工业职业技术学院石油与化学工程系,南宁530001 [2]广西地矿测试研究中心,南宁530023 [3]广西师范学院化学与生命科学学院,南宁530001

出　　处：《中国调味品》2010年第9期87-90,共4页China Condiment

基　　金：广西教育厅科研项目(200911LX502);广西工业职业技术学院课题(桂工职院科研2009001005号)

摘　　要：文章以石油醚为溶剂,用索氏法从草豆蔻中提取挥发油,然后通过气相-质谱(GC-MS)联用手段对挥发油的主要化学成分进行分析,以峰面积归一化法确定各组分的相对含量;结果从草豆蔻挥发油的15个色谱峰中鉴定出14种成分,占挥发油总含量的98.16%,其主要成分依次为α-石竹烯、α-法尼醇、石竹烯、3-苯基-2-丁酮、δ-荜澄茄烯等。在元素分析方面,用ICP-MS/ICP-AES法测定草豆蔻中的19个无机元素,元素的含量顺序为Mg>P>Ca>Mn>Al>Fe>Zn>B>Ba>Cu>Sr>Ni=Ti>Pb>Co>V>Cr>Li>Cd。Volatile oil from Alpinia katsumadai hayata was extracted by Soxhelt method with petroleum ether as solvent,and analysised by GC-MS（gas chromatography-mass spectrometry）,15 peaks were separated,of which 14 compounds were identified,accounted for 98.16% of the oil,with α-Caryophyllene,α-Farnesol,Caryophyllene,3-Phenyl-2-butanone,δ-Cadinene,as the main ingredient.The contents of 19 inorganic elements were determined by using ICP-MS and ICP-AES technique.There were MgPCaMnAlFeZnBBaCuSrNi = TiPbCoVCrLiCd.

关 键 词：草豆蔻 挥发油 索氏法 化学成分 气相-质谱 ICP-MS ICP-AES 无机元素 

分 类 号：TS255.19[轻工技术与工程—农产品加工及贮藏工程]