过氧化钙的制备研究  

The Research on Preparation of Calcium Peroxide

作　　者：张顺成[1,2] 

机构地区：[1]河北理工大学化工与生物技术学院,河北唐山063000 [2]唐山市建材产品质量监督检验站,河北唐山063000

出　　处：《河北化工》2010年第9期19-20,54,共3页Hebei Chemical Industry

摘　　要：研究了氢氧化钙-氯化铵-双氧水法生产过氧化钙的工艺过程和影响因素。通过单因素实验,得到制备过氧化钙的最佳工艺条件为反应温度26℃、反应时间35 min、稳定剂偏硅酸钠用量14%、双氧水浓度15%、氢氧化钙过量50%、氯化铵用量n(NH4Cl)∶n(Ca(OH)2)=1.5。In this paper,calcium peroxide was produced by calcium hydroxide and ammonium chloride with hydrogen perox-ide.The factors of influencing calcium peroxide were investigated.The optimum conditions were determined by the mono-factor experiments.The results showed that reaction time was 35 min,reaction temperature was 26 ℃,stabilizer dosage was 14%,hydrogen peroxide concentration was 9%,excessive amount of calcium hydroxide was 50%,excessive amount of ammonium chloride was n（NH4Cl）∶n（Ca（OH）2）=1.5.

关 键 词：过氧化氢 氢氧化钙 氯化铵 过氧化钙 稳定剂 

分 类 号：TQ132.32[化学工程—无机化工]