采用分离集成技术提取废弃烟叶中精品茄尼醇  

Isolation of refined solanesol from abandon tobacco by separation integrated technology

作　　者：顾正桂[1,2] 刘玲[1] 顾美娟[1,2] 林军[1,2] 

机构地区：[1]南京师范大学江苏萃取分离工程技术研究中心,江苏南京210097 [2]江苏沿江化工资源开发研究院,江苏南京210097

出　　处：《化学工程》2010年第10期136-140,共5页Chemical Engineering(China)

基　　金：江苏省高校科研成果产业化推进项目(JH08-7)

摘　　要：提供了一种从烟叶浸膏中提取精品茄尼醇的分离集成技术,设计了一系列该分离技术中所需的实验设备,包括球形夹套式皂化萃取装置、超低温离心结晶装置及连续中压柱层析分离装置。采用分离集成技术及设备,成功将质量分数为20%左右的烟叶浸膏经过皂化萃取,得到质量分数为59%左右的半成品茄尼醇,再通过结晶得到质量分数为80%左右的高纯度茄尼醇,最终通过柱层析和重结晶得到质量分数为95.5%的精品茄尼醇,整个实验过程的得率为70%。克服了现有技术中能耗大、溶剂污染严重等缺点。A separation integrated technology for isolating refined solanesol from tobacco extracts was provided.Some experimental installations applied in the separation integrated technology were designed,including saponification and extraction installation,cryogenic centrifugation crystallization installation and continuous medium pressure chromatography separation installation.With the separation integrated technology and installations,semi-finished products solanesol（mass fraction 59%） was successfully got from tobacco extracts（mass fraction 20%） by saponification and extraction,again,high purity solanesol（mass fraction 80%） by crystallization,finally,competitive products solanesol（mass fraction 95.5%） by chromatography and recrystallization.The yield of the whole experiment is 70%,overcoming disadvantages in the existing technology such as huge consumption of energy,heavy pollution of solvents.

关 键 词：茄尼醇 分离 皂化萃取 结晶 柱层析 

分 类 号：TS49[农业科学—烟草工业]