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机构地区:[1]湖北省农科院农业测试与科技信息中心,湖北武汉430064 [2]湖北省农药检定管理所,湖北武汉430070
出 处:《农药科学与管理》2010年第4期40-42,共3页Pesticide Science and Administration
摘 要:本文介绍了以5%OV-101色谱柱固定相,邻苯二甲酸二丁酯为内标物,用FID检测器利用程序升温对噻嗪·异丙威25%可湿性粉剂2种组分的气相色谱分离测定方法。结果表明,噻嗪酮和异丙威的标准偏差分别为0.026、0.047,变异系数分别为0.32%、0.28%,噻嗪酮的回收率为99.34%~101.03%,异丙威的回收率为99.16%~101.47%。该方法简便、快捷、准确。An analytical method for the determination of buprofezin, isoprocarb 25% WP by GC was described in this paper. The samples were separated in a column packed with OV-101 and detected by flame ionization detector. The results showed that the standard deviations were 0.026 and 0.047, the coefficients of variation were 0.32% and 0.28%, the average recoveries were 99.34%-101.03%% and 99.16%-101.47% for buprofezin and isoprocarb respectively. This method is convenient, rapid and accuracy.
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