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机构地区:[1]辽宁石油化工大学石化学院,辽宁抚顺113001
出 处:《日用化学工业》2010年第6期418-421,共4页China Surfactant Detergent & Cosmetics
摘 要:以Co/SBA-15为催化剂,52号石蜡为原料,制备氧化石蜡,并考察了乳化温度、乳化时间、乳化剂用量等因素对乳化效果的影响。结果表明,HLB值为9.3的复配型非离子乳化剂具有较好的乳化效果。较适宜的乳化条件为:乳化剂质量分数为7.3%(占总量)、乳化时间55 min、乳化温度75℃、乳化用水质量分数为69.96%(占总量)。制得的乳液具有稳定性好、保质期长、无毒无味、色泽好等优点。石蜡氧化后乳化性能有很大提高,乳化剂用量减少。Adopting Co/SBA - 15 as catalyst, 52 # paraffin wax as raw material, oxidized paraffin wax was prepared. The influences of the emulsification temperature, emulsification time, emulsifier dosage and other factors on the effect of the emulsification were investigated. The results showed that the blended nonionic emulsifier of HLB value of 9.3 displays good performance. The appropriate emulsification conditions are as follows : dosage of emulsifier 7.3% ( mass fraction of total emulsified mixture), emulsification time 55 min, emulsification temperature 75℃, water to be emulsified with mass fraction of total emulsified mixture 69.96%. The emulsion has advantages of good stability, long shelf life, non - toxic and tasteless, and good color. From the comparison of the emulsion performance of the raw material wax with the wax after oxidation treatment, it can be seen that the emulsion performance of oxidized paraffin wax was improved considerably and the dosage of emulsifier is reduced.
分 类 号:TE626.88[石油与天然气工程—油气加工工程]
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