相转移催化法合成N-1-芳基,-乙酰基,-羧甲氧烷基苯并三唑  

PHASE TRANSFER CATALYTIC SYNTHESIS OF N 1 ARYL , ACETYL AND CARBOXYMETHOXYALKYL BENZOTRIAZOLES

作　　者：谢筱娟[1] 程林[1] 李友华 

机构地区：[1]安徽师范大学化学系

出　　处：《安徽师范大学学报（自然科学版）》1999年第2期152-154,共3页Journal of Anhui Normal University(Natural Science)

基　　金：安徽省教育委员会基金

摘　　要：报道了以聚乙二醇为相转移催化剂合成１－（１－Ｈ－苯并三唑基）－２，４－二硝基苯，１－［α－（１－Ｈ－苯并三唑基）］乙酰苯并三唑和两个１－（１－Ｈ－苯并三唑基）烷氧乙酸．本法反应时间短，产率令人满意．初步的生物活性测定结果表明，化合物Ⅰ。Synthesis of the 1 (benzotriazol 1 yl) 2,4 dinitrobenzene, 1 [α (benzotriazol 1 yl) acetyl benzotriazole and 1 (benzotriazol yl) alkoxy acetic acid in the presence of phase transfer catalyst has been reported. The method has advantages of good yield, short reaction time and easy operation. Their biological activities were tested. The results shoued that Ⅰ Ⅲ a and Ⅲ b possess very strong inhibition activities.

关 键 词：芳基 乙酰基 羧甲氧烷基 苯并三唑 相转移催化 

分 类 号：O626.26[理学—有机化学]