HPLC测定蒙药清热止痛三味汤散中秦皮乙素的含量  

Mongolian Heat Pain Shamisen Soup Powder Aesculetin Determination

作　　者：屈爱桃[1] 孙超[1] 刘翔宇[1] 李乐娟[1] 白明安图[1] 张静[1] 

机构地区：[1]内蒙古医学院,呼和浩特010059

出　　处：《中国实验方剂学杂志》2011年第2期87-88,共2页Chinese Journal of Experimental Traditional Medical Formulae

摘　　要：目的:建立高效液相色谱法测定清热止痛三味汤散中秦皮乙素的含量的方法。方法:采用高效液相色谱法测定秦皮乙素的含量。结果:秦皮乙素在0.168～2.94μg线性关系良好(r=0.999 5),平均回收率为98.04%,RSD 0.74%(n=6)。结论:该方法简便易行、重现性好。可用于清热止痛三味汤散中秦皮乙素含量测定。Objective：To establish a high performance liquid chromatography heat pain shamisen soup powder Aesculetin content approach.Method：Uses the highly effective liquid phase chromatography to determine Esculetin the element the content.Result：Aesculetin in the range of 0.168-2.94 μg good linear relationship（r=0.999 5,n=5）.The average recovery was 98.04%,RSD 0.74%（n=6）.Conclusion：The method is simple,accurate and reproducible.Can be used to heat pain shamisen soup powder Aesculetin content.

关 键 词：清热止痛三味汤散 秦皮乙素 高效液相色谱法 

分 类 号：R284.1[医药卫生—中药学]