叉枝鸦葱黄酮类化合物提取工艺的研究  

Study on Extraction Technique of Total Flavonoids from Scorzonera Divaricata

作　　者：马国财[1,2] 陈义磊[1,2] 王小强[2] 白红进[1,2] 

机构地区：[1]新疆生产建设兵团塔里木盆地植物资源保护与利用重点实验室 [2]塔里木大学生命科学学院,新疆阿拉尔市843300

出　　处：《光谱实验室》2011年第1期286-291,共6页Chinese Journal of Spectroscopy Laboratory

基　　金：新疆维吾尔自治区群体创新项目(No.XJEDU2005G07);塔里木大学校长基金重点项目(TDZKZD05002)

摘　　要：采用均匀实验设计对叉枝鸦葱总黄酮的提取工艺进行了研究。主要考察乙醇浓度、提取时间、料液比及提取次数等4个因素对提取率的影响,优选出合理的提取工艺。结果表明水浴回流提取法最佳提取工艺为:15%乙醇、料液比为1:34、提取时间为45min、提取次数为3次;超声-微波协同提取法最佳提取工艺为:30%乙醇、料液比为1:36、提取时间为41min、提取次数为3次。通过比较两种提取方法,超声-微波协同提取法具有省时、节能、操作方便等优点。The extraction technique of total flavonoids from Socrzonera divricata by uniform design was studied.The effects of ethanol concentration,extraction time,the ratio of material to solvent and extraction number were observed.The result showed that the best extraction technique of water bath reflux method was as follows：15% ethanol,the ratio of material to solvent of 1：34,extraction time of 45min,and extraction for 3 times.The best extraction technique of ultrasonic-microwave synergistic was as follows：30% ethanol,the ratio of material to solvent of 1：36,extraction time of 41min,and extraction for 3 times.By comparison,ultrasonic-microwave method has advantages of saving time,lower energy consumption and facility of manipulation.

关 键 词：叉枝鸦葱 总黄酮 提取工艺 

分 类 号：O657.32[理学—分析化学]