静态顶空GC-MS法测定化妆品中的甲醛  

Determination of formaldehyde in cosmetic products by headspace gas chromatography-mass spectrometry

作　　者：杨雪梅[1] 周枝凤[1] 马安德 万新祥[2] 

机构地区：[1]南方医科大学公共卫生与热带医学学院卫生检测中心,广州510515 [2]南方医科大学药学院,广州510515

出　　处：《分析试验室》2011年第2期92-94,共3页Chinese Journal of Analysis Laboratory

摘　　要：建立了化妆品中甲醛的快速检测方法。采用自动顶空GC-MS法,优化顶空条件,选用叔丁醇作为内标,甲醛浓度在5.6～560μg/g范围内,线性良好(r=0.9995)。甲醛的最低检出浓度为0.6μg/g,回收率90.23%～108.79%,RSD在4.3%～9.4%之间。A selective, rapid and simple method was developed for the quantitative determination of formaldehyde in cosmetic products. A headspace gas chromatography-mass spectrometry was employed for the analysis of formaldehyde in cosmetic; products. The conditions of headspace has been tested and optimized. Tertbutanol was used as an internal standard. The linear range of formaldehyde was from 5.6 μg/g to 560 μg/g （ r = 0. 9995 ） , the detection limit of formaldehyde was 0. 6 μg/g. The range of recovery was from 90. 23 % to 108.79% , and RSDs were from 4.3% to 9.4%.

关 键 词：甲醛 化妆品 顸空 气相色谱-质谱法 

分 类 号：O657.63[理学—分析化学]