益康药酒的质量标准研究  

Study on Quality Standard of Yikang Medicinal Liquor

作　　者：马晓星[1] 韩翠艳[1] 朱丹 王建明[3] 王岩松[3] 

机构地区：[1]齐齐哈尔医学院,黑龙江齐齐哈尔161006 [2]齐齐哈尔中医院,黑龙江齐齐哈尔161006 [3]黑龙江中医药大学,哈尔滨150040

出　　处：《中国实验方剂学杂志》2011年第5期101-104,共4页Chinese Journal of Experimental Traditional Medical Formulae

摘　　要：目的:建立益康药酒的质量控制标准。方法:采用薄层色谱法(TLC)对处方中的淫羊藿、巴戟天、锁阳、当归、补骨脂、山茱萸进行定性鉴别,采用HPLC测定淫羊藿苷的含量。结果:TLC鉴别专属性强、重现性好。淫羊藿苷的线性范围0.246～0.574μg(r=0.999 9),平均加样回收率99.71%,RSD 0.47%。结论:本方法能有效地控制益康药酒的质量。Objective：To establish quality standard of Yikang medicinal liquor. Method： TLC was used to identify Epimedy , gorinda officinalis , Cynomorium ,Angelica sinensis , Psoralea fruit and Cornus officinalis ; HPLC was used to determine the content of icariin. Result： The reproducibility and specialization of the TLC method were good. The linear range of icariin was 0. 246-0. 574 μg （r = 0. 999 9） by HPLC, and the average recovery rate was 99.71% with relative standard deviation of 0.47%. Conclusion： The method can control the quality of Yikang Medicinal Liquor.

关 键 词：益康药酒 质量标准 TLC HPLC 

分 类 号：R284.1[医药卫生—中药学]