有机颜料中间体N,N′-双乙酰乙酰基2-甲基-5-氯代-1,4-苯二胺的合成  

Synthesis of Organic Pigmet Intermidiate N, N' - bisacetylaceto - 2 - methyl - 5 - chloro -1,4- Phenylenediamine

作　　者：魏荣宝[1] 李绍武[1] 吕金魁[1] 郑嗣华[1] 马德珍 

机构地区：[1]天津理工学院化工系,300191

出　　处：《化工时刊》1999年第10期30-33,共4页Chemical Industry Times

摘　　要：以对氯甲苯为原料,经硝化,还原,N-酰化、水解、乙酰乙酰化反应,制成有机颜料中间体N,N′-双乙酰乙酰基2-甲基-5-氯代-1,4-苯二胺。对影响反应的诸因素进行了讨论。A organic pigment intermidiate N,N' - bisacetylaceto - 2-methyl - 5 - chloro - 1,4 - phenylenediamine was synthesized, through by nitration, reduction, N - acctylation, N - acetylacetylation, using 4 - chloromethyl benzene as first material. Some experimantal parameters were discussed.

关 键 词：有机颜料 双乙酰乙酰基 甲基 苯二胺 中间体 

分 类 号：TQ246.31[化学工程—有机化工] TQ616.8