毛细管气相色谱法分析甲基丙烯酸甲酯中的阻聚剂  

Analysis of polymerization inhibitor in methyl methacrylate by capillary gas chromatography

作　　者：卢志琴[1] 刘海珍[1] 文明[1] 

机构地区：[1]张家港出入境检验检疫局,江苏张家港215600

出　　处：《化学工程师》2011年第2期28-29,36,共3页Chemical Engineer

摘　　要：本文采用毛细管气相色谱法测定甲基丙烯酸甲酯中的阻聚剂——2,4-二甲基-6-叔丁基苯酚,操作简便,结果准确。实验选择了最佳汽化温度、柱温和载气流速。外标法定量,回收率可达99%～102%,变异系数为0.6%。The polymerization inhibitor in methyl methacrylate,2,4-dimethyl-6-tert-butyl phenol was analyzed by capillary gas chromatography.The method is simple and accurate.The best vaporization temperature,column temperature and flow rate of carrier gas were selected.The recovery is 99%-102% rationed by external standard method.The coefficient of variation is 0.6%.

关 键 词：甲基丙烯酸甲酯 气相色谱 2 4-二甲基-6-叔丁基苯酚 

分 类 号：O657.8[理学—分析化学]