复方颈康丸质量标准研究  

Study on the Quality Standard of Compound Jinkang Pill

作　　者：叶福媛[1] 张钰泉[1] 林梅[1] 王健英[1] 

机构地区：[1]上海中医药大学,上海201203

出　　处：《黑龙江医药》2011年第1期27-29,共3页Heilongjiang Medicine journal

摘　　要：目的:建立复方颈康丸质量标准。方法:采用薄层色谱法对复方颈康丸中黄芪、防己进行定性鉴别研究;采用HPLC法对复方颈康丸中特征性成分青藤碱进行含量测定。结果:黄芪、防己薄层鉴别斑点清晰,无干扰。青藤碱在0.4-4.0μg范围内线性关系良好,回归方程为y=1207X+1.0185,平均回收率为98.65%,RSD为1.199%。结论:该方法简便,准确,重现性好,可作为复方颈康丸质量控制的方法。Objective：To establish the quality standard of Compound Jinkang Pill.Methods：Radix Astragali and Radix Stephaniae Tetrandrae in Compound Jinkang Pill were identified by TLC.determination was determined by HPLC.Results：The spots on TLC plates were clear and no interference.Sinomenine had the linear range of 0.4～4.0μg（r=0.9998,n=5）.The average recovery was 98.65%（RSD=1.199,n=6）.Conclusion：The method is easy,accurate and reproducible.It can be used for quality control of Compound Jinkang Pill.

关 键 词：复方颈康丸 青藤碱 质量标准 

分 类 号：R284.1[医药卫生—中药学]