电子电器产品中含溴阻燃剂的萃取  

Extraction of Brominated Flame Retardants in Electrical and Electronic Products

作　　者：罗群[1] 陈洪伟[1] 梁志辉[1] 范洪波[1] 

机构地区：[1]东莞理工学院化学与环境工程学院,广东东莞523808

出　　处：《广东化工》2011年第3期118-119,142,共3页Guangdong Chemical Industry

基　　金：东莞市科技计划项目(NO.2008108101018)

摘　　要：电子电器产品中含溴阻燃剂的萃取方法有索氏萃取、自动索氏萃取、超声波萃取、超临界萃取、微波辅助萃取和快速溶剂萃取等。文章通过对比索氏萃取、微波辅助萃取和快速溶剂萃取并结合高效液相色谱法测定电子塑料产品中的含溴阻燃剂,探讨合适的萃取方法,实验结果表明,索氏萃取效果最好,回率91.8%~98.4%,RSD%=5,满足检测要求。There exist extraction methods such as Soxhlet Extraction（SE）,automatic Soxhlet Extraction,Ultrasonic Extraction（UE）,Supercritical Fluid Extraction（SFE）,Microwave Assisted Extraction（MAE） and Accelerated Solvent Extraction（ASE） for brominated flame retardants in electrical and electronic products.By comparing the Soxhlet extraction,microwave assisted extraction and accelerated solvent extraction and HPLC determination for brominated flame retardants,we tried to find a appropriate extraction method.As a result,Soxhlet extraction was found to be the best in this work,with the recoveries of 91.8%~98.4%,RSD% = 5,meeting the testing requirements.

关 键 词：含溴阻燃剂 电子电器产品 萃取方法 

分 类 号：O65[理学—分析化学]