热等静压法制备高立方织构的镍基合金复合基带  

Fabrication of Ni-based alloy composite substrate with high cube texture using hot isostatic presses method

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作  者:邱火勤[1] 索红莉[1] 寇生中[1,2] 马麟[1] 田辉[1] 刘敏[1] 袁冬梅[1] 王营霞[1] 

机构地区:[1]北京工业大学材料科学与工程学院,北京100124 [2]兰州理工大学材料科学与工程学院,兰州730050

出  处:《中国有色金属学报》2011年第7期1632-1638,共7页The Chinese Journal of Nonferrous Metals

基  金:国家重点基础研究发展计划资助项目(2006CB601005);国家高技术研究发展计划资助项目(2009AA032401);国家自然科学基金资助项目(50771003;50802004);北京市自然科学基金资助项目(2092006);教育部新世纪优秀人才资助项目(39009001201002)

摘  要:采用热等静压(HIP)法制备芯层为Ni-12%W(Ni12W,摩尔分数)合金、外层为Ni-5%W(Ni5W,摩尔分数)合金的Ni5W/Ni12W/Ni5W 3层复合初始坯锭;采用压延辅助双轴织构技术(RABiTSTM)通过直接冷轧及再结晶退火获得Ni5W/Ni12W/Ni5W复合基带;采用X射线四环衍射技术(XRD)及背散射电子衍射技术(EBSD)对复合基带表面冷轧及再结晶织构进行分析。结果表明:冷轧复合基带表面形成较强的铜型形变织构,再结晶退火后复合基带表面形成锐利的立方织构,其立方织构含量达到99.1%(≤10°),与商业用Ni5W合金基带水平相当。A tri-layer composite alloy ingot was fabricated by hot isostatic presses(HIP) method,in which the outer layer is Ni-5%W(Ni5W,mole fraction) alloy and the inner layer is Ni-12%W(Ni12W,mole fraction) alloy.The composite ingot was cold-rolled using the process of rolling assisted biaxially textured substrate(RABiTSTM) technology and annealed to obtain the Ni5W/Ni12W/Ni5W composite substrate with high cube texture.The cold rolling and the recrystallization textures on the surface of the as-obtained composite substrate were studied systematically by X-ray and EBSD measurements.The results show that a strong deformation copper-type texture is obtained in the cold rolled composite substrate,and a sharp cube texture is formed on the surface of Ni5W/Ni12W/Ni5W composite substrate after a recrystallization annealing process.The percentage of the cube orientated grain within a misorientation angle of 10° is as high as 99.1%,which is in the same level as that of the commercial Ni5W tape.

关 键 词:镍基复合基带 热等静压 铜型织构 立方织构 

分 类 号:TM26[一般工业技术—材料科学与工程]

 

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