纳米金属酞菁MPc(M=Fe,Co,Ni,Cu和Zn)的合成与表征  

Preparation and characterization of nanoscle metal phthalocyanines MPc(M=Fe,Co,Ni,Cu,Zn)

作　　者：宁波[1,2] 郭增彩[2] 柯福波[2] 王井峰[2] 邵长路[2] 

机构地区：[1]长春职业技术学院食品与生物技术分院,吉林长春130021 [2]东北师范大学化学学院,吉林长春130024

出　　处：《东北师大学报（自然科学版）》2011年第3期80-83,共4页Journal of Northeast Normal University(Natural Science Edition)

基　　金：国家自然科学基金资助项目(50572014;50972027)

摘　　要：采用溶剂热方法以邻苯二甲腈为原料、乙二醇为溶剂在反应釜中合成了各种形貌的Fe,Co,Ni,Cu和Zn纳米金属酞菁化合物,并对它们进行了电子扫描电镜、XRD、红外光谱及紫外-可见光谱表征.结果表明,产品纯度高,产率大,形貌独特.Fe,Co,Ni,Cu,Zn＇s phthalocyanine compound nanostructure has been successfully obtained by a facile ethylene glycol solvent-thermal synthetic route.It was characterized by SEM,XRD,IR,and UV-vis spectrum.It was indicated that the obtained metal phthalocyanines with high yields and purity had the unipue morphology and structure.

关 键 词：金属酞菁 溶剂热 纳米 合成 表征 

分 类 号：O614[理学—无机化学]