3-[2,6-二氯-4-(3,3-二氯烯丙氧基)苯氧基]丙基吡唑-5-甲酰胺类衍生物的合成及杀虫活性  

Synthesis and Insecticidal Activity of 3-[2,6-Dichloro-4-(3,3-dichloroallyloxy) phenoxy] Propyl Pyrazole-5-carboxamide Derivatives

作　　者：马海军[1] 张雁南[1] 倪珏萍[1] 

机构地区：[1]江苏省农药研究所股份有限公司,南京210047

出　　处：《现代农药》2011年第5期16-20,23,共6页MODERN AGROCHEMICALS

基　　金：国家"十一五"科技支撑计划(2006BAE01A01-3);江苏省自然科学基金(BK2009026)

摘　　要：以3-[2,6-二氯-4-(3,3-二氯烯丙氧基)苯氧基]丙胺和5-吡唑甲酸衍生物为原料,设计并合成了19个未见报道的3-[2,6-二氯-4-(3,3-二氯烯丙氧基)苯氧基]丙基吡唑-5-甲酰胺类衍生物。目标化合物的结构经IR和1HNMR测定确认。初步杀虫活性测试结果表明,该类化合物对鳞翅目害虫具有较好的杀虫活性。Nineteen novel 3-[2,6-dichloro-4-（3,3-dichloroallyloxy）phenoxy]propyl pyrazole-5-carboxamide derivatives were synthesized by the reaction of 3-[2,6-dichloro-4-（3,3-dichloroallyloxy） phenoxy] propan-1-amine with pyrazole-5-carboxylic acid derivatives.All compounds were confirmed by IR and 1H NMR.The preliminary bioassay showed that the compounds exhibited good activity against lepidopterous pests.

关 键 词：二氯代丙烯类 吡唑-5-甲酰胺 合成 杀虫活性 

分 类 号：TQ453.2[化学工程—农药化工]