间羟基-N,N-二乙基苯胺的分析方法研究  

A Study on Analysis Method of m-HydroxyN,N-diethylaniline

作　　者：季浩[1] 

机构地区：[1]沈阳化工研究院有限公司,沈阳110021

出　　处：《染料与染色》2011年第5期55-56,24,共3页Dyestuffs and Coloration

摘　　要：采用气相色谱对间羟基-N,N-二乙基苯胺及其有机杂质进行分离,用峰面积归一化法进行定量分析。通过气相色谱-质谱联用仪对间羟基-N,N-二乙基苯胺及其有机杂质进行分离并定性,给出了各化合物的结构式。使用精密度数据对分析方法进行了评价。m-Hydroxy-N,N-diethylaniline and its organic impurities were separated by gas chromatography,and their contents were quantified by peak area normalization method.m-Hydroxy-N,N-diethylaniline and its organic impurities were separated and qualitatively analyzed by GC-MS.The structural formulae of m-hydroxy-N,N-diethylaniline and impurities were presented.The analysis method was evaluated by the data of precision.

关 键 词：间羟基-NN -二乙基苯胺 气相色谱 峰面积归一化法 

分 类 号：TQ207.4[化学工程—有机化工]