氟乙酰胺、氢氰酸混合杀鼠剂中毒检验的研究  

Study on Toxic Inspection of Mice-killing Mixture of Flurocetamide and HCN

作　　者：任荣光 

机构地区：[1]福建省南平地区公安处,南平353000

出　　处：《福建分析测试》1994年第3期138-142,共5页Fujian Analysis & Testing

摘　　要：本文描述了应用衍生化色谱技术,同时检測生物体内的氟乙酰胺、氢氰酸。用五氟溴苄和氯胺T分别作为氟乙酰胺和氢氰酸衍生化试剂,衍生化产物用GC/ECD检测,在Parapak—QS+3％DC—200混合填充柱上,均得到良好分离,平均提取回收率>81%。动物实验和案例检验证明方法准确、可靠、灵敏度高。可成功地检测中毒患者或致死者体内的氢氰酸和氟乙酰胺的含量,并适用于临床抢救监测。A simultaneous determination of fluoracetamide and HCN in biological samples was described using derivatization GC. The derivatization reagents were pentafluorobromotoluene and chloramine T. The resultants were separated on Parapak—QS+3%DC—200 package column and deteoted with ECD. The recovery was over 81 %. It was accurate, reliable and sensitive, can be used for clinical purpose.

关 键 词：FLUOROACETAMIDE HCN biological SAMPLES 

分 类 号：R595.4[医药卫生—内科学]