甲亚胺H-酸分光光度法测定固体废弃物中的硼  

Determination of Boron in Solid Waste by Azomethine-H spetrophotometric method

作　　者：汪曼洁 何伟彪 黄俊华 冯献芳 王志杰 

机构地区：[1]深圳市环境监测中心站,广东518000

出　　处：《环境与发展》2011年第11期110-112,共3页Environment & Development

摘　　要：采用不同浸提剂对固体废物中的硼进行浸提并用甲亚胺-H酸分光光度法进行分析,结果表明,pH=2.64±0.05的冰醋酸水溶液提取率最高。探讨了显色时间、pH值和金属离子等主要因素对测定的影响,选择了最佳实验条件,加标回收率在87%～103%之间。通过与ICP-AES方法比对结果表明,该方法准确可靠。Various extraetants were applied for extraction of Boron from solid waste, and the obtained extracts were analyzed by Azomethine-H spetrophotometric melhod. The result showed that aqueous acetic acid with pH=2.64 ± 0.05 has better extraction rate than others. The effeets of developing time, plt value, metal ion and operating conditions were studied. The results gained under optimum condilion indicated that addition recovery was between 87%- 103%. Comparison with ICP-AES method shows that this method is reliable and the accmacy is suitable.

关 键 词：硼 固体废弃物 浸提 甲亚胺-H酸 分光光度法 

分 类 号：X833[环境科学与工程—环境工程]