以碳酸二甲酯为酯化试剂的绿色合成方法  

Green Synthetic Method Study on Dimethyl Carbonate Esterification Reagent

作　　者：杨涛[1] 王金[1] 杨健[1] 杨波[1] 

机构地区：[1]昆明理工大学生命科学与技术学院

出　　处：《光谱实验室》2012年第1期338-340,共3页Chinese Journal of Spectroscopy Laboratory

摘　　要：以碳酸二甲酯为酯化试剂,以DMSO为溶剂.碳酸钾为去酸剂,合成了两个羧酸甲酯类化合物。结构经红外光谱和~1H NMR确证,表明碳酸二甲酯可以作为一种绿色、环保的酯化试剂,具有广泛的应用前景。Two kinds carboxylate compounds were synthesized with dimethyl carbonate as esterification reagent,DMSO as solvent and potassium carbonate as disacidify reagent.The structures of the products were characterized by ~1H NMR and IR spectrum.Dimethyl carbonate can be used as a kind of green and environmental esterification reagent,that has a wide range of applications prospect.

关 键 词：绿色合成方法 碳酸二甲酯 甲基化 酯化 

分 类 号：O657.33[理学—分析化学] O657.2[理学—化学]