Synthesis and Crystal Structure of 8-Methyl-7-(3-nitrophenyl)-10-phenyl-10,11-dihydrochro-meno[4,3-b]pyrazolo[4,3-e]pyridin-6-(7H)-one  

作　　者：林志兰 游新奎 张雪利 高原 

机构地区：[1]College of Chemistry and Chemical Engineering,Shenzhen University

出　　处：《Chinese Journal of Structural Chemistry》2012年第1期57-60,共4页结构化学（英文）

基　　金：Project supported by the National Natural Science Foundation of China (No. 81071144);Natural Science Foundation of Guangdong Province (No. 9451806001002961)

摘　　要：The title compound（C26H18N4O4） has been synthesized via a three-component reaction and it was characterized by means of IR and 1H NMR.Its crystal and molecular structures were determined by X-ray diffractometry.It belongs to the triclinic system,space group P1 with a = 7.7288（15）,b = 11.168（2）,c = 12.645（3） ,α = 107.02（3）,β = 90.85（3）,γ = 101.93（3）°,V = 1017.9（3） 3,Mr = 450.44,Z = 2,Dc = 1.470 g/cm3,λ = 1.54178 ,μ = 0.836 mm-1,F（000） = 468,the final R = 0.0488 and wR = 0.1180.A total of 11903 reflections were collected,of which 3642 were independent（Rint = 0.0377） and 3025 were observed with I 2σ（I）.The title compound（C26H18N4O4） has been synthesized via a three-component reaction and it was characterized by means of IR and 1H NMR.Its crystal and molecular structures were determined by X-ray diffractometry.It belongs to the triclinic system,space group P1 with a = 7.7288（15）,b = 11.168（2）,c = 12.645（3） ,α = 107.02（3）,β = 90.85（3）,γ = 101.93（3）°,V = 1017.9（3） 3,Mr = 450.44,Z = 2,Dc = 1.470 g/cm3,λ = 1.54178 ,μ = 0.836 mm-1,F（000） = 468,the final R = 0.0488 and wR = 0.1180.A total of 11903 reflections were collected,of which 3642 were independent（Rint = 0.0377） and 3025 were observed with I 2σ（I）.

关 键 词：multicomponent reaction coumarin derivatives crystal structure 

分 类 号：O626.21[理学—有机化学]