原子荧光光谱法测定赛霉安阴道栓中朱砂含量  

Determination of cinnabar in Saimeian vaginal suppositories by AFS

作　　者：林兰婷 黄汉明 庄波阳[2] 

机构地区：[1]福建省福州市中医院,福州350001 [2]福建省药品检验所,福州350001

出　　处：《海峡药学》2012年第3期70-71,共2页Strait Pharmaceutical Journal

摘　　要：目的建立利赛霉安阴道栓中朱砂的含量测定方法。方法采用原子荧光光谱法测定样品中钠的含量。结果朱砂在2.514～7.542ng.mL-1范围内线性关系良好,相关系数为0.9991;回收率在101.0%～105.1%,RSD为1.5%。结论该方法简单、快速、准确;能很好地用于赛霉安阴道栓中朱砂的质量控制。OBJECTIVE To establish a method to determine cinnabar in Saimeian vaginal suppositories.METHODS The content of cinnabar in the samples was determinated by the method of hydride generation-atomic fluorescence spectrometer（AFS）.RESULTS The good linear relation was determined as 2.514~7.542ng·mL-1in cinnabar by AFS with a regression coefficient of 0.9991.The average recovery rate was 101.0%~105.1%;The relative standard deviation was 1.5%.CONCLUSION The method was simple,rapid and accurate,and can be used for quality control of cinnabar in SaiMeiAn vaginal suppositories.

关 键 词：原子荧光光谱法 赛霉安阴道栓 朱砂 含量测定 

分 类 号：R927.2[医药卫生—药学]