Synthesis and Crystal Structure of 2-(4-Chlorophenyl)-1,4,5-triphenyl-1H-imidazole  

作　　者：Ali Mohammad Amani Kazem Barati 

机构地区：[1]Young Researchers Club,Shiraz Branch,Islamic Azad University [2]Young Researchers Club,Yasooj Branch,Islamic Azad University

出　　处：《Chinese Journal of Structural Chemistry》2012年第4期574-576,共3页结构化学（英文）

基　　金：supported by Islamic Azad University,Yasuj Branch

摘　　要：The compound 2-（4-chlorophenyl）-1,4,5-triphenyl-1H-imidazole（1,C27H19ClN2） has been synthesized and its crystal structure was determined by single-crystal X-ray diffraction.The crystal of 1 belongs to the triclinic system,space group P with a = 10.3350（19）,b = 10.238（2）,c = 11.201（2） ,α = 85.957（16）,β = 83.148（15）,γ = 66.467（15）°,V = 1078.5（4） 3,Mr = 406.89,Z = 2,F（000） = 422,Dc = 1.257 g/cm3,μ = 0.193 mm-1,T = 298（2） K,S = 1.092,R = 0.0702 and wR = 0.1258.The imidazole ring system is planar and makes a dihedral angle of 40.3° with the chlorobenzene ring.The compound 2-（4-chlorophenyl）-1,4,5-triphenyl-1H-imidazole（1,C27H19ClN2） has been synthesized and its crystal structure was determined by single-crystal X-ray diffraction.The crystal of 1 belongs to the triclinic system,space group P with a = 10.3350（19）,b = 10.238（2）,c = 11.201（2） ,α = 85.957（16）,β = 83.148（15）,γ = 66.467（15）°,V = 1078.5（4） 3,Mr = 406.89,Z = 2,F（000） = 422,Dc = 1.257 g/cm3,μ = 0.193 mm-1,T = 298（2） K,S = 1.092,R = 0.0702 and wR = 0.1258.The imidazole ring system is planar and makes a dihedral angle of 40.3° with the chlorobenzene ring.

关 键 词：crystal structure IMIDAZOLE triclinic system 

分 类 号：O627.3[理学—有机化学]