N-丁基-3,6-二乙酰基咔唑的合成及表征  

Synthesis and Characterization of N-Butyl-3,6-Diacetyl Carbazole

作　　者：董金龙[1] 张永斌[2] 张改玲[1] 张丽[1] 

机构地区：[1]太原师范学院化学系,太原市黄陵路19号030031 [2]山西大学化学化工学院,太原市坞城路92号030006

出　　处：《光谱实验室》2012年第3期1827-1829,共3页Chinese Journal of Spectroscopy Laboratory

基　　金：2011年度山西省高校科技开发项目(20111122)

摘　　要：以咔唑为合成原料,在相转移催化剂作用下合成N-丁基咔唑,作为电子给体和共轭桥中心,乙酰氯作为端基电子受体,合成了V型化合物:N-丁基3,6-二乙酰基咔唑。其结构经IR,1H NMR和GC-MS表征。N-butyl-carbazole that was as electron donor and conjugate bridge center,was prepared under the phase transfer catalyst effect with carbazole as composition raw meterial and acetylchloride as the end group electronic receptor.Base on the conditions,the V-type compounds,N-butyl-3,6-diacetyl carbazole,were synthesized.The structures of the compounds were charecterized by IR,1H NMR and GC-MS.

关 键 词：咔唑 合成 表征 

分 类 号：O625.65[理学—有机化学] O657.61[理学—化学]