高压均质技术对低熔点玻璃粉的细化及烧结性能的影响  

Effect of Refinement Process Condition and Sintering Property on the Low Melting Point Glass Powder by High-pressure Homogenization Technology

作　　者：张念椿[1] 熊俊军[1] 丁恩勇[1] 

机构地区：[1]华南理工大学高分子研究所,广州510641

出　　处：《无机材料学报》2012年第8期855-859,共5页Journal of Inorganic Materials

基　　金：国家自然科学基金(50873038;21075043)~~

摘　　要：利用羧甲基纤维素(CMC)作为低熔点玻璃粉水分散液的防沉剂,用高压均质机对玻璃粉进行细化处理,使其粒度减小.探讨了不同高压均质时间对玻璃粉的粒度大小和烧结性能的影响;结果表明:在相同的压强下(50 MPa),高压均质时间越长则玻璃粉粒度越小、粒度分布范围越窄,其软化温度和烧结温度也越低.因此可以利用高压均质技术来降低玻璃粉的粒度,从而降低玻璃粉的软化温度和烧结温度.Using carboxymethyl cellulose （CMC） as an anti-settling agent of low melting point glass powder aqueous dispersion, the high-pressure homogenizer can refine glass powder particle to reduce their size. Different high-pressure homogenized time affected on glass powder＇s particle size and the sintering property. Under the same pressure （50 MPa） a longer high-homogeneous time gets smaller particle size and narrows particle size distribution. And the softening temperature and sintering temperature are also lower. The results show that the high-pressure homogenizer techniques can be used to reduce the particle size of the glass powder, so that the softening temperature and sintering temperature will be lowered.

关 键 词：玻璃粉 均质时间 烧结性能 粒度 

分 类 号：TB34[一般工业技术—材料科学与工程]