含呋喃环双酰腙类化合物的合成与结构表征  

Synthesis and Structure Characteristics of Bi-Hydrazones with Furan Ring

作　　者：陈桐滨[1] 赖意君[1] 邱玉英[1] 

机构地区：[1]韩山师范学院化学系,广东省潮州市桥东521041

出　　处：《光谱实验室》2012年第5期2878-2880,共3页Chinese Journal of Spectroscopy Laboratory

基　　金：韩山师范学院青年科学基金(LQ200805);韩山师范学院"大学生创新性实验计划"项目

摘　　要：以3,4-呋喃二羧酸为原料,经酯化、肼解合成3,4-呋喃二酰肼,再与芳香醛、酮类化合物发生缩合反应,合成6个含呋喃环双酰腙类化合物。通过1H NMR、FTIR、MS对它们的结构进行了表征。3,4-furan di-acylhyrazines prepared through esterification and hydrazinolysis of furan 3,4-dicarboxylic acid,then reacted with aromatic aldehydes or ketones compounds by the reaction of condensation reaction,then Bi-hydrazones with furan rings compound was synthesized.The structures of compounds were characterized by 1H NMR,FTIR and MS.

关 键 词：呋喃 双酰腙 合成 表征 

分 类 号：O657.61[理学—分析化学]