屏风生脉胶囊中3种药材的鉴别与五味子醇甲的测定  

Study on the quality standard of Pingfeng Shengmai capsule

作　　者：王慧 袁祥慧 邓开英 

机构地区：[1]重庆市食品药品检验所,重庆400015

出　　处：《华西药学杂志》2012年第5期566-568,共3页West China Journal of Pharmaceutical Sciences

摘　　要：目的完善屏风生脉胶囊的质量标准。方法采用TLC法鉴别方中人参、黄芪、五味子;采用HPLC测定方中五味子醇甲的含量。结果 TLC鉴别色谱特征的斑点明显;五味子醇甲0.2256～2.8200μg与峰面积的线性关系良好(r=0.9999),平均加样回收率为101.5%,RSD=1.4%(n=6)。结论所用方法专属性强、重复性好,可用于屏风生脉胶囊的质量控制。OBJECTIVE To improve the quality standard of Pingfeng Shengmai capsule.METHODS Ginseng Radix er Rhizoma,Astragali Radix and Schisandrae chinensis Fructus were identified by TLC and the content of schisandrin was determined by HPLC.RESULTS The developed TLC spots was quite clear.The calibration curve of schisandrin was linear within 0.2256-2.8200 μg（r=0.9999）.The average recovery was 101.5% with the RSD of 1.4%（n=6）.CONCLUSION The established TLC and HPLC method are specific,reproducible and suitable for the quality control of Pingfeng Shengmai capsule.

关 键 词：屏风生脉胶囊 质量标准 人参 黄芪 五味子 五味子醇甲 

分 类 号：R917[医药卫生—药物分析学]