6-甲酰基香豆素的合成及提纯  

Synthesis and Purification of 6-Formylcoumarin

作　　者：孔祥文[1] 张源[1] 张静[1] 梁媛[1] 周秀丽[1] 

机构地区：[1]沈阳化工大学应用化学学院,沈阳110142

出　　处：《科学技术与工程》2012年第30期7993-7994,共2页Science Technology and Engineering

基　　金：辽宁省教育科学"十一五"规划立项课题(JG09DB112)资助

摘　　要：以6-甲基香豆素为原料,经NBS溴代得6-溴甲基香豆素,再经Sommelet反应得到6-甲酰基香豆素。研究了一种新的6-甲酰基香豆素提纯方法。产物经红外光谱、熔点确认结构。6-Formylcoumarin was prepared from 6-methylcoumarin through NBS bromination and Sommelet re-action. A new method for purification of the title product was also studied. The structure of the product is character-ized by m.p. and IR.

关 键 词：6-甲酰基香豆素 NBS溴代 Sommelet反应 合成 

分 类 号：O626.411[理学—有机化学]