双检测器串联色谱柱分析六味地黄丸  

Analyse of Liuwei Dihuang Pills by HPLC with Series Double-detector and Double-column

作　　者：邢占芬[1] 成洪达[1,2] 张维冰[2,3] 

机构地区：[1]山东万杰医学院,山东淄博255213 [2]大连依利特分析仪器公司,辽宁大连116023 [3]中国科学院大连化学物理研究所,辽宁大连116023

出　　处：《福建分析测试》2012年第6期45-48,共4页Fujian Analysis & Testing

基　　金：国家自然科学基金(20675083)

摘　　要：对高效液相色谱系统进行了改造并用于中药六味地黄丸的分析。紫外检测器与蒸发光散射检测器串联以提高峰容量;升高分析温度串联色谱柱以增加柱效。结果显示,紫外检测器共检测到156个峰,蒸发光散射检测器检测到195个峰,其中41个色谱峰为可以认证的共有峰,所构建的系统非常适宜于中草药指纹图谱的研究。Liuwei Dihuang Pills was analyzed by reformed HPLC system. In order to increase peak volume, ultraviolet detector and Evaporative Light Scattering Detector were used in series; For high column efficiency, two columns connected under high analysis temperature. The number of peak ultraviolet detector detected was 156 and Evaporative Light Scattering Detector was 195, among which 41 peaks were mutual. The system was very suitable for the research of Chinese Traditional Medicine fingerprint spectrum.

关 键 词：高效液相色谱 紫外检测器 蒸发光散射检测器 串联色谱柱 六味地黄丸 

分 类 号：O657.72[理学—分析化学]