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出 处:《北方药学》2012年第12期4-5,共2页Journal of North Pharmacy
摘 要:目的:建立痔疮外洗剂的质量标准。方法:采用薄层色谱法鉴别大黄,紫外分光光度法测定总生物碱的含量。结果:薄层斑点清晰,阴性样品无干扰;平均回收率为102.6%,RSD为0.64%。结论:该方法准确、可靠,重现性好,可有效控制本制剂的质量。Objective:To establish the quality standard on Pile Lotion. Methods:TLC identified Rhubarb, the contents of total alkaloids was determined by UV-spectrometry .Results:The TLC spots was fairly clear, negative samples were no interference and the average reeovery was 102.6%, RSD 0.64%.Conclusions:The established method was accurate, reliable and good reproducible,it can control the quality of Pile lotion.
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