醋狼毒饮片质量标准研究  

Study on Quality Standard of Vinegar Backed Euphorbia Ebracteolata

作　　者：邓英君[1] 庄果[2] 汪兰云[2] 李俊松[2] 蔡宝昌[2] 葛乃贵 

机构地区：[1]南京市中医院,南京210001 [2]南京中医药大学江苏省中药炮制重点实验室,南京210029 [3]江苏省海安针灸推拿学校,江苏南通226600

出　　处：《中国实验方剂学杂志》2012年第23期98-101,共4页Chinese Journal of Experimental Traditional Medical Formulae

基　　金：国家公益性行业专项基金项目(200807039);南京中医药大学中药学一级学科开放课题(2011ZYX2-011)

摘　　要：目的:制订醋狼毒饮片的质量标准。方法:收集炮制10批醋狼毒饮片,对水分、总灰分、酸不溶性灰分、浸出物进行测定,并以狼毒乙素含量为指标进行含量测定。结果:拟定醋狼毒饮片水分不得超过9.12%,总灰分不得超过6.50%,酸不溶性灰分不得超过1.09%,醇溶性浸出物不少于7.70%,狼毒乙素含量不少于0.038%。结论:初步建立醋狼毒饮片量化质控标准评价体系。Objective： To revise and improve the quality standard of vinegar backed E. ebracteolata. Method： 10 batches of vinegar backed Euphorbia ebracteolata were investigated with TLC. Moisture content, total ash, acid-insoluble ash and extractum were explored. The content of ebracteolata cpd B was determined by HPLC. Result： The quality standard was preliminarily formulated as follows： the moisture content should not pass 9.12%. Total ash should not pass 6.50%. Acid-insoluble ash should not pass 1.09%. Alcohol-soluble extractive should not lower than 7.70%. The content of ebracteolata cpd B should not lower than 0. 038%. Conclusion： Quality control quantization evaluation system of processed E. ebracteolata slice is preliminarily established.

关 键 词：醋狼毒 质量标准 含量测定 

分 类 号：R284.1[医药卫生—中药学]