β-萘氧基酞菁钴/二氧化锡复合材料的制备及表征  

Preparation and characterization of β-naphthyloxy-Cobalt Phthalocyanine/SnO_2 Nanocomposite

作　　者：金永茂[1] 任卉蕾[1] 孙季如[1] 尹彦冰[1] 

机构地区：[1]齐齐哈尔大学化学与化学工程学院,黑龙江齐齐哈尔161006

出　　处：《高师理科学刊》2012年第6期43-45,共3页Journal of Science of Teachers＇College and University

基　　金：黑龙江省普通高等学校青年学术骨干支持计划项目(1153G052)

摘　　要：采用原位合成的方法制备β-萘氧基酞菁钴/二氧化锡复合材料,利用UV,IR,XRD,TG对产物进行表征.结果表明,复合材料在紫外光谱中出现了酞菁特征吸收,并且出现Q带的红移现象,红外光谱中出现了M-O的振动吸收峰,在XRD谱图中显现出SnO2晶粒变小,说明-萘氧基酞菁钴与二氧化锡之间具有一定的相互作用.β-naphthyloxy-Cobalt Phthalocyanine/SnO2 composite was synthesized by in-situ method. The prepared product was characterized by means of UV, IR, XRD and TG methods. The experimental results indicate that the UV spectrum brings about moving to more longer wavelength in its characteristic absorption Q belt. The vibration absorption peaks of M-O appreared in IR spectrum, the size of crystal particals has become smaller than before, all that show in the complex β-naphthyloxy-Cobalt Phthalocyanine and SnO2 were linked with partial chemical bond.

关 键 词：原位合成 复合材料 二氧化锡 

分 类 号：TQ423.11[化学工程]