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作 者:Wu-bin Gao Yun-han Ling Xu Liu Jia-lin Sun
机构地区:[1]School of Materials Science and Engineering, University of Science and Technology Beijing, Beijing 100083, China [2]Department of Materials Science and Engineering, Tsinghua University, Beijing 100084, China
出 处:《International Journal of Minerals,Metallurgy and Materials》2012年第12期1142-1148,共7页矿物冶金与材料学报(英文版)
基 金:supported by the National Natural Science Foundation of China (Nos.NSAF10876017, NSAF10776017, and91023037)
摘 要:A simple and new point contact tungsten trioxide (WO3) sensor, which can be prepared by the oxidation of tungsten filaments via in-situ induction heating, likely detects low concentration (ppm level) environmental pollutants such as NO2. X-ray diffraction (XRD) and field emission scanning electron microscopy (FE-SEM) were applied to characterize the phase and the microstructure of the samples, respec-tively. It was found that the synthesized WO3 films exhibited a monoclinic phase and were composed of hierarchical microcrystals and nanocrystals. The point contact WO3 sensor (W-WO3-W) showed rectifying characteristics and an ideal sensing performance of about 110 C. A single semicircle in Nyquist plots was recorded by electrochemical impedance spectroscopy (EIS) at a relatively low temperature of 150 C but faded away above 200 C, which revealed that the sensing process was governed by a determining factor, i.e., grain boundaries at the contact site.A simple and new point contact tungsten trioxide (WO3) sensor, which can be prepared by the oxidation of tungsten filaments via in-situ induction heating, likely detects low concentration (ppm level) environmental pollutants such as NO2. X-ray diffraction (XRD) and field emission scanning electron microscopy (FE-SEM) were applied to characterize the phase and the microstructure of the samples, respec-tively. It was found that the synthesized WO3 films exhibited a monoclinic phase and were composed of hierarchical microcrystals and nanocrystals. The point contact WO3 sensor (W-WO3-W) showed rectifying characteristics and an ideal sensing performance of about 110 C. A single semicircle in Nyquist plots was recorded by electrochemical impedance spectroscopy (EIS) at a relatively low temperature of 150 C but faded away above 200 C, which revealed that the sensing process was governed by a determining factor, i.e., grain boundaries at the contact site.
关 键 词:gas sensors tungsten trioxide metal oxide semiconductors thin fills MICROCRYSTALS NANOCRYSTALS electrochemical impedancespectroscopy (EIS)
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