N,N’-二芳基-吡啶二甲酰胺和N,N’-双-吡啶甲酰胺烃类配体的合成及其结构表征  

SYNTHESIS AND STRUCTURE CHARACTERIZATION OF THE LIANDS CONTAINING PYRIDINECARBOXAMIDE AND PYRIDINEDICARBOXAMIDE

作　　者：戚建英[1] 马红霞[1] 杨启云[2] 李泽珍 邓立生 李贤均[1] 

机构地区：[1]四川大学化学学院有机金属络合催化研究所,成都610064 [2]云南师范大学化学系,昆明650031 [3]中国科学院成都有机所,成都610061

出　　处：《四川大学学报（自然科学版）》2000年第3期414-419,共6页Journal of Sichuan University(Natural Science Edition)

基　　金：中国科学院兰州化学物理研究所 0 SS0重点实验室基金

摘　　要：合成了含 N,N’-二芳基 -吡啶二甲酰胺和 N,N’-双 -吡啶甲酰胺烃类的九种配体 ,它们的结构经 UV,MS,IR,1HNMR及元素分析所确证 .比较了两种合成方法的优缺点 。ligands, which included N,N’diphenyl2,6pyridinedicarboxamide,N,N’ bis (pmethoxyphenyl)2,6pyridinedicarboxamide,N,N’bis(pmethylphenyl)2,6pyridinedicarbox amide,N,N’bis(pchlorophenyl)2,6pyridinedicarboxamide,N,N’bis(pnitrophenyl)2,6pyridinedicarboxamide,N,N’bis(2pyridinecarboxamide)1,2beneze,N,N’bis(2pyridinecarboxamide)1,2ethane,N,N’bis(2pyridinecarboxamide)1,4butane,N,N’bis(2pyridinecarboxamide)1,6hexane have been synthesized.The structure of these ligands was characterized by UV,MS,IR, -1HNMR and elemental analysis.Two synthetic methods have been compared and the synthetic conditions have been investigated.

关 键 词：合成 二芳基-吡啶二甲酰胺 双吡啶甲酰胺类配体 

分 类 号：O626.32[理学—有机化学] O641.4[理学—化学]