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机构地区:[1]上海市中医医院,上海200040 [2]上海医药工业研究院,上海200040
出 处:《中医药导报》2013年第2期97-99,共3页Guiding Journal of Traditional Chinese Medicine and Pharmacy
摘 要:目的:建立三黄止痒搽剂的薄层定性鉴别方法。方法:采用HPTLC法,以不同展开系统分别对处方中黄柏、黄芩、大黄、苦参进行薄层定性鉴别。结果:HPTLC的斑点清晰、分离度较好。处方样品中斑点与对照品中斑点Rf值一致,阴性无干扰。结论:所建立的方法对方中的药材可准确、快速地进行定性检测,可用于三黄止痒捈剂的质量控制。Objective: To establish a method of high performance thin layer chromatography (HPTLC) for identifying the qualitation of Sanhuang liniment. Methods: Identified the Amur Corktree Bark, Baikal Skullcap Root, Rhubarb and Lightyellow Sophora Root in the prescription of Sanhuang Liniment by different development system with HPTLC. Results: The spots appeared clear and the resolution was satisfactory. The Rf values of spots of prescription samples were consistent with those of reference substance. There is no negative interference. Conclusion: The method is proved to be sensitive and precise, and can be used for the quality control of Sanhuang liniment.
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