蒽油中金属钠、铁和铜含量测定原子吸收光谱法的研究  

Determination of Sodium、Iron and Copper content in Anthracene Oil- Atomic absorption spectrometric method

作　　者：陈信悦[1] 吴建国[1] 孙延伟[1] 于孝展[1] 田元红[1] 

机构地区：[1]辽宁出入境检验检疫局技术中心,辽宁大连116001

出　　处：《福建分析测试》2013年第2期48-53,共6页Fujian Analysis & Testing

摘　　要：试样在蒸发皿中,先用小火慢慢加热灰化,至大部分挥发物挥发后,将蒸发皿置于高温炉中灰化后,用盐酸溶解,采用火焰原子吸收光谱法测定蒽油中的钠、铁和铜含量。实验表明,钠、铁和铜含量在0～5 mg/L范围内线性关系良好,相关系数γ=0.999,该法回收率93%～104%,能满足进出口蒽油检验的要求。The samples were in the crucible,then heated it slowly with softfire and ashed it ,after evaporated of most of evaporating matte~ ,put the crucible in the oven and ashed it,then disolved it with HCI solution. Determination fo Sodium,Iron and Copper content in Anthracene Oils with Atomic AbsorPtion Spectrometric Method （ Flame Method ）.The result shows,in the range of 0-5mg/1,the liner relation of the content of Iron and Copper is good,corresponding factor u =0.999,and its recovery ratio is 93- 104%,can make the requirement of the inspection of Import and Export Anthracene Oils.

关 键 词：蒽油 钠 铁 铜 原子吸收光谱法 

分 类 号：TQ662.13[化学工程] O657.3[理学—分析化学]