清胃黄连丸的质量标准研究  

Study on Quality Standard of Qingwei Huanglian Pilll

作　　者：孔庆兰[1] 安君 赵晶晶[1] 宋新波[1] 张丽娟[1] 

机构地区：[1]天津中医药大学,天津300193 [2]天津中一制药有限公司

出　　处：《现代中药研究与实践》2013年第1期56-58,共3页Research and Practice on Chinese Medicines

摘　　要：目的完善清胃黄连丸的质量标准。方法采用显微鉴定法进行定性鉴别,采用高效液相色谱法进行含量测定。结果处方中13味中药粉末显微特征明显;丹皮酚在0.007 92mg-0.047 52mg线性关系良好(r=0.999 9),平均回收率为101.51%,RSD值为1.6%。结论本试验方法准确度、精密度、稳定性、重复性良好,可以用于清胃黄连丸的质量控制。Objective To perfect a method of the quality standard for Qingwei Huanglian Pill. Methods Microscopic identification was used to identify the whole 13 Chinese medicines in Qingwei Huanglian Pill, HPLC was used for content determination of Paeonol. Results The microscopic characteristics of the whole 13 Chinese medicines in Fangfeng Tongsheng Pill were distinct. Paeonol had a good linear relationship at 0.007 92 mg- 0.047 52 mg.And the average recovery was 101.51%, the RSD was 1.6%. Conclusion This method was accurate, sensitive, stable and reproducible. It could be used to control the quality of Qipgwei Huanglian Pill.

关 键 词：清胃黄连丸 质量标准 显微鉴定法 高效液相色谱法 丹皮酚 

分 类 号：R927.1[医药卫生—药学]