三草酸合铁(Ⅲ)酸钾制备实验的改进探索  

Conditions Optimization for the Preparation of Potassium Ferrioxalate

作　　者：刘冬莲[1] 刘娅萍[1] 刘爽[1] 张宁[1] 

机构地区：[1]唐山师范学院化学系,河北唐山063000

出　　处：《唐山师范学院学报》2013年第2期17-19,共3页Journal of Tangshan Normal University

基　　金：唐山师范学院教改项目(2012001016)

摘　　要：根据三草酸合铁(Ⅲ)酸钾K3[Fe(C2O4)3].3H2O制备实验的实际情况,对反应温度、H2O2去除时间、Fe(OH)3溶解温度、KHC2O4加入方式进行了探究。通过优化实验过程,可得到粒度较大的翠绿色晶体,提高了产率和实验教学效果。The experimental conditions were optimized for the preparation of potassium ferrioxalate according to the practice of experiments, and the temperature, the remove time of H202, the solubolity temperature of Fe（OH）3 and the addition of oxalic were explored in the preparation of potassium ferrioxalate. By optimizing experimental process, we can obtain the emerald crystal grains in improved process, and the yield was increased. The effectiveness of experimental teaching was ameliorated.

关 键 词：三草酸合铁(III)酸钾 制备 实验改进 

分 类 号：G642.0[文化科学—高等教育学]