参归仁颗粒质量标准研究  

Study on Quality Standand of Shenguiren Granule

作　　者：谢玉[1] 冯俭[2] 席小兰[1] 李树翠[1] 贝圆[1] 

机构地区：[1]成都中医药大学,四川成都610072 [2]成都中医药大学附属医院,四川成都610072

出　　处：《亚太传统医药》2013年第4期26-27,共2页Asia-Pacific Traditional Medicine

摘　　要：目的:建立参归仁颗粒的质量标准。方法:用TLC法对人参、当归进行定性鉴别;用高效液相色谱法测定人参中人参皂苷Rb1、Re、Rg1的含量。结果:TLC图谱特征明显,人参皂苷Rb1、Re、Rg1分别在0.212～2.12mg/mL、0.2156～2.156mg/mL、0.206～2.06mg/mL范围内线性关系良好(r=0.9999),平均回收率及RSD均达到标准。结论:该方法简便可行,重复性好,能有效控制参归仁颗粒的质量。Objective：To establish the quality standard for Shenguiren Granules. Methods：Ginseng and Angelica were qualitative ly identified by TLC. To establish a method for the measure of ginsenoside Rbl, Re, Rgl in Ginseng with HPLC. Results： The chromatographic characteristics for TLC identification were distinct . The linearity ranges for ginsenoside Rbl, Re, Rgl were 0.212 2.12mg（r=0.9999）,0.2156 2.156mg （r=0.9999） and 0.206--2.06mg（r=0.9999） ,respectively. The average recoveries and RSD were comply with the requirements. Conclusion： The used method is feasible with good reproducibility and can control the quality of the Shenguiren granules effectively.

关 键 词：参归仁颗粒 人参 薄层色谱法 高效液相色谱法 质量标准 

分 类 号：R283[医药卫生—中药学]