Multicomponent reactions for the synthesis of functionalized 1,4-oxathiane-3-thiones under microwave irradiation in water  

作　　者：Zinatossadat Hossaini Faramarz Rostami-Charati Samereh Seyfi Mehdi Ghambarian 

机构地区：[1]Department of Chemistry,Qaemshahr Branch,Islamic Azad University [2]Department of Chemistry,Facualty of Science,Gonbad Kavous University [3]Department of Chemistry,Oaemshahr Branch,Islamic Azad University [4]Department of Chemistry,Karaj Branch,Islamic Azad University

出　　处：《Chinese Chemical Letters》2013年第5期376-378,共3页中国化学快报（英文版）

摘　　要：A series of substituted l,4-oxathiane-3-thione derivatives were synthesized via one-pot multicomponent reactions of nitromethane,carbon disulfide and oxiranes in the presence of Et;N in water as the solvent under microwave irradiation.Particularly valuable features of this method include high yields of products,broad substrate scope,short reaction time and straightforward procedure.A series of substituted l,4-oxathiane-3-thione derivatives were synthesized via one-pot multicomponent reactions of nitromethane,carbon disulfide and oxiranes in the presence of Et_3N in water as the solvent under microwave irradiation.Particularly valuable features of this method include high yields of products,broad substrate scope,short reaction time and straightforward procedure.

关 键 词：OXIRANE NITROMETHANE Carbon disulfide 1 4-Oxathiane Three-component reaction 

分 类 号：O621.3[理学—有机化学]