乙酸乙酯标准物质的制备  

Preparation of ethyl acetate standard material

作　　者：张卫平[1] 蒋锦锋[2] 张兵[3] 陆明华[1] 朱书秀[1] 

机构地区：[1]浙江中烟工业有限责任公司技术中心,杭州市科海路118号310024 [2]中国烟草总公司郑州烟草研究院 [3]浙江省烟草专卖局(公司)烟草质量监督检测站,杭州市将军路9号310001

出　　处：《中国烟草学报》2013年第2期23-28,共6页Acta Tabacaria Sinica

基　　金：国家烟草专卖局标准制修订项目"卷烟用纸分析用挥发性有机化合物混合溶液标准物质"(合同号:2011B054)

摘　　要：为解决卷烟包装纸残留挥发性有机化合物分析中缺少乙酸乙酯标准物质问题,利用高纯乙酸乙酯试剂为原料,严格控制配制和封装过程,研制出乙酸乙酯溶液标准物质,并对其进行了均匀性检验和稳定性考察。7家实验室对该标准物质进行了合作定值,结果为1.02 mg/mL,扩展不确定度为0.03 mg/mL,符合国家二级标准物质技术要求。Ethyl acetate solution certified reference material was prepared under strict control of preparation and packaging processes with high purity Ethyl acetate reagent as raw material. Homogeneity and stability were measured using GC-FID method. Concentration value of the reference material was 1.02 mg/mL, with an expanded uncertainty of 0.03 mg/mL based on cooperation analysis of 7 laboratories. Results indicated that the certified reference material met all technical requirements of national secondary reference material.

关 键 词：卷烟包装纸 乙酸乙酯 标准物质 

分 类 号：TS47[农业科学—烟草工业]