肉苁蓉药材质量标准的研究  

A Study on Quality Standard for Herba Cistanches

作　　者：张思巨[1] 刘丽[1] 张淑运[1] 扈继萍[1] 王宏洁[1] 

机构地区：[1]中国中医研究院中药研究所,北京100700

出　　处：《中国中药杂志》2000年第6期359-361,共3页China Journal of Chinese Materia Medica

基　　金："九五"国家重点攻关项目! (96 90 3 0 2 0 2 )

摘　　要：目的 :制订肉苁蓉药材的质量标准。方法 :建立 5种活性成分类叶升麻苷、松果萄苷、肉苁蓉苷A、甜菜碱和甘露醇的TLC定性鉴别及类叶升麻苷的RP HPLC测定方法。结果 :14个药材和 11个饮片样品的薄层色谱斑点清晰 ,专属性强 ;麦角甾苷在 0 .15～ 1.2 0 μg线性关系良好 ,平均回收率 98.0 % ,RSD 0 .95 %。 结论 :本法可作为肉苁蓉药材的质量控制标准。Objective:To establish the quality standard for Herba Cistanches.Method:A qualitative identification method by TLC was established for five kinds of active components(acteoside,echinacoside,cistanoside A,betaine and mannitol) and RP HPLC was used to quantify the acteoside contents.Result:Qualitative and quantitative analyses were carried out for fourteen kinds of Herba Cistanches and eleven kinds of Yinpian .This method is accurate,reliable and of good separability and reproducibility.Conclusion:This method can be applied as standard for the quality control of cistanche deserticola. [

关 键 词：肉苁蓉 类叶升麻苷 松果萄苷 肉苁蓉苷A 

分 类 号：R282.710.3[医药卫生—中药学]